WE ARE COMMITTED TO REPORTING THE LATEST FORESTRY ACADEMIC ACHIEVEMENTS

Volume 39 Issue 2
Nov.  2019
Article Contents
Turn off MathJax

ZHAO Chun-chao, YANG Xue-bing, XU Ming, YANG Lei, MO Kai-lin. GC-MS Analysis of Volatile Oil from Leaves of Cinnamomum pedunculatum from Sichuan[J]. Journal of Sichuan Forestry Science and Technology, 2018, 39(2): 26-29. doi: 10.16779/j.cnki.1003-5508.2018.02.006
Citation: ZHAO Chun-chao, YANG Xue-bing, XU Ming, YANG Lei, MO Kai-lin. GC-MS Analysis of Volatile Oil from Leaves of Cinnamomum pedunculatum from Sichuan[J]. Journal of Sichuan Forestry Science and Technology, 2018, 39(2): 26-29. doi: 10.16779/j.cnki.1003-5508.2018.02.006

GC-MS Analysis of Volatile Oil from Leaves of Cinnamomum pedunculatum from Sichuan


doi: 10.16779/j.cnki.1003-5508.2018.02.006
More Information
  • Received Date: 2017-12-21
  • The technology of solvent-free microwave-assisted extraction (SFME) was compared with hydrodistillation (HD) by the extraction of volatile oils from the Sichuan Cinnamomum pedunculatum leaves, and the GC-MS technology was used in separation and identification of the main constituents. The percentage of the individual volatile component was calculated by the normalization method of peak area. And the conclusions showed that the main components of the volatile oils were similar, nevertheless the yield of the individual constituent was different by the two extraction methods; solvent-free microwave-assisted extraction (SFME) was a more efficiency extraction technology compared with the HD, especially in the extraction time (40 min versus 200 min) and the yield of volatile oils (6.50 mL·kg-1 versus 5.46 mL·kg-1). SFME had the characteristics of efficiency, low cost and no pollution,and it should be widely generalized in the practical application.
  • 加载中
  • [1] 毕淑峰,杨梦雅,刘羽.野生天竺桂挥发油化学成分的GC-MS分析[J].黄山学院学报,2013,15(5):66~69.
    [2] 蔡建秀,吴文杰,陈晓梅.天竺桂叶挥发油的提取及抗炎活性研究[J].时珍国医国药, 2008,29(6):26~30.
    [3] 舒康云,陶永元,陈成东,等.天竺桂精油的提取及成分分析[J].中南林业科技大学学报, 2014,34(1):107~111.
    [4] 王平,张萍,侯茂,等.天竺桂水提液对油樟悬浮细胞黄酮类积累的影响[J].生物学通报,2012,47(10):39~40.
    [5] 福建省科学技术委员会《福建植物志》编写组.福建植物志(第2卷)[M].福州:福建科学技术出版社,1982:103~104.
    [6] 蔡建秀,尤祖卿,黄晓东,等.天竺桂挥发油化学成分及抑菌活性研究[J].热带亚热带植物学报,2006,14(5):403~408.
    [7] 黄晓东,黄晓昆,张娴,等.天竺桂叶精油的含量动态、化学成分及体外抗菌活性[J].中国农学通报,2010,26(4):182~188.
    [8] 黄晓冬,蔡建秀,邱凯宁.天竺桂挥发油镇痛、抗癫痫的作用[J].中国医院药学杂志,2011,31(20):1676~1678.
    [9] 申鸽,彭映辉,秦巧慧,等.天竺桂叶精油成分分析及其对蚊虫的毒杀作用[J].中南林业科技大学学报,2010,30(9):132~136.
    [10] 王月亮,陈凯,李慧,等.石菖蒲无溶剂微波提取工艺的优化研究及其挥发性成分的GC-MS分析[J].中草药,2016,47(3):414~419.
    [11] 王研,杨美丹,李建亮,等.自制微波辅助无溶剂萃取装置及GC/MS分析白玉兰花挥发油[J].质谱学报,2009,30(4):244~249.
    [12] 刘伟.蓝桉叶精油微波无溶剂法提取及抗氧化、抗菌活性研究[D].东北林业大学硕士论文2015:6.
    [13] 傅小红.微波无溶剂提取的应用进展[J].广东化工,2014,41(9):123~124.
    [14] 吴恒,吴雨凇,殷沛沛,等.西双版纳小叶杜鹃花挥发性成分研究[J].江西农报, 2015,27(5):71~74.
  • 加载中
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索

Article views(474) PDF downloads(9) Cited by()

Related
Proportional views

GC-MS Analysis of Volatile Oil from Leaves of Cinnamomum pedunculatum from Sichuan

doi: 10.16779/j.cnki.1003-5508.2018.02.006
  • Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, Heilongjiang, China;Sichuan Academy of Forestry, Chengdu 610081, Sichuan, China

Abstract: The technology of solvent-free microwave-assisted extraction (SFME) was compared with hydrodistillation (HD) by the extraction of volatile oils from the Sichuan Cinnamomum pedunculatum leaves, and the GC-MS technology was used in separation and identification of the main constituents. The percentage of the individual volatile component was calculated by the normalization method of peak area. And the conclusions showed that the main components of the volatile oils were similar, nevertheless the yield of the individual constituent was different by the two extraction methods; solvent-free microwave-assisted extraction (SFME) was a more efficiency extraction technology compared with the HD, especially in the extraction time (40 min versus 200 min) and the yield of volatile oils (6.50 mL·kg-1 versus 5.46 mL·kg-1). SFME had the characteristics of efficiency, low cost and no pollution,and it should be widely generalized in the practical application.

Reference (14)

Catalog

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return