Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk

ZHENG Yu-chuan; WANG Chao; CHENG Jian-wei; WANG Zhi-peng; YANG Lin

doi:10.16779/j.cnki.1003-5508.2018.01.005

Volume 39 Issue 1

Nov. 2019

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ZHENG Yu-chuan, WANG Chao, CHENG Jian-wei, WANG Zhi-peng, YANG Lin. Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk[J]. Journal of Sichuan Forestry Science and Technology, 2018, 39(1): 22-26. doi: 10.16779/j.cnki.1003-5508.2018.01.005

Citation:

ZHENG Yu-chuan, WANG Chao, CHENG Jian-wei, WANG Zhi-peng, YANG Lin. Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk[J]. Journal of Sichuan Forestry Science and Technology, 2018, 39(1): 22-26. doi: 10.16779/j.cnki.1003-5508.2018.01.005

Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk

doi: 10.16779/j.cnki.1003-5508.2018.01.005

More Information

Sichuan Academy of Forestry, Chengdu 610081, China;Rongxian Forestry Bureau, Rongxian 43100;Chengdu 610068, China

Received Date: 2017-12-05

Abstract

Walnut is one of the important forest products in our country.Polyphenolic compounds extracted from Walnut green husk were abundant and healthy to the human body.However because of carelessly discarded husk,environment became increasingly worsened.This paper reviewed the research progress of biological activity,separation and purification of the polyphenols of walnut green husk,and looked forward to the research and application in the future,aiming to provide some thoughts in scientific research and the application of walnut green husk's polyphenolic resources for the purpose of promoting the walnut industry.
- Walnut green husk;
- Research progress;
- Polyphenols;
- Biological activity;
- Separation and purification

References

[1]	郗荣庭,张毅萍.中国核桃[M].中国林业出版社,1992.
[2]	姚焕英,唐静成,张鞍灵,等.核桃属植物化学成分及生物活性研究[J].西北植物学报,2003,23(9):1650~1655.
[3]	周正.世界主要用材树种概论[M].中国林业出版社,1997.
[4]	Silva B M,Andrade P B,Valentão P,et al.Quince (Cydonia oblonga Miller) fruit (pulp,peel,and seed) and jam:antioxidant activity.[J].Journal of Agricultural & Food Chemistry,2004,52(15):4705.
[5]	Pulido R,Bravo L,Saura-Calixto F.Antioxidant activity of dietary polyphenols as determined by a modified ferric reducing/antioxidant power assay.[J].J Agric Food Chem,2000,48(8):3396~3402.
[6]	Stampar F,Solar A,Hudina M,et al.Traditional walnut liqueur-cocktail of phenolics.[J].Food Chemistry,2006,95(4):627~631.
[7]	杜旭,李玉文,倪雁,等.中药青核桃镇痛作用研究与展望[J].中国中药杂志,2000,25(1):7~10.
[8]	董再冉.核桃酒治疗腹痛和胃痛[J].中国医刊,1966(7 ).
[9]	黄织女.青核桃泡酒治肺癌[J].老同志之友,2014(9):61.
[10]	林开敏,叶发茂,林艳,等.酚类物质对土壤和植物的作用机制研究进展[J].中国生态农业学报,2010,18(5):1130~1137.
[11]	何强,姚开,石碧.植物单宁的营养学特性[J].林产化学与工业,2001,21(1):80~85.
[12]	王全杰,李超,王纯,等.核桃青皮中单宁的类型及含量测定[J].皮革与化工,2011,28(3):25~27.
[13]	Binder R G,Benson M E,Flath R A.Eight 1,4-naphthoquinones from Juglans[J].Phytochemistry,1989,28(10):2799~2801.
[14]
[15]	Cushnie T P T,Lamb A J.Antimicrobial activity of flavonoids.International Journal of Antimicrobial Agents[J].2005(26):343~356
[16]	曲中原,邹翔,管小玉,等.青龙衣不同萃取部位化学成分GC-MS分析[J].中草药,2010,41(10):1625~1626.
[17]	Colaric M,Veberic R,Solar A,et al.Phenolic Acids,Syringaldehyde,and Juglone in Fruits of Different Cultivars of Juglans regia L.[J].Journal of Agricultural & Food Chemistry,2005,53(16):6390~6396.
[18]
[19]	张建斌,柳军玺,查飞,等.青龙衣的化学成分研究[J].中草药,2009,40(6):847~849.
[20]	Oliveira I,Sousa A,Ferreira I C,et al.Total phenols,antioxidant potential and antimicrobial activity of walnut (Juglans regia L.) green husks.[J].Food & Chemical Toxicology An International Journal Published for the British Industrial Biological Research Association,2008,46(7):2326.
[21]	Keskin D,Ceyhan N,Ugur A.Chemical composition and in vitro antimicrobial activity of walnut (Juglans regia) green husks and leaves from West Anatolia[J].Journal of Pure & Applied Microbiology,2012,6(2):583~588.
[22]	Pereira J A,Oliveira I,Sousa A,et al.Bioactive properties and chemical composition of six walnut (Juglans regia L.) cultivars.[J].Food & Chemical Toxicology,2008,46(6):2103~2111.
[23]	Yieit D,Yigit N,Aktas E,et al.Antimicrobial activity of walnut (Juglans regia L.)[J].Turk Microbiol Soc,2009,1~2(39):7~11.
[24]	Clark A M,Jurgens T M,Hufford C D.Antimicrobial activity of juglone.[J].Phytotherapy Research,1990,4(1):11~14.
[25]	Costa R M,Magalhães A S,Pereira J A,et al.Evaluation of free radical-scavenging and antihemolytic activities of quince (Cydonia oblonga) leaf:A comparative study with green tea (Camellia sinensis)[J].Food & Chemical Toxicology An International Journal Published for the British Industrial Biological Research Association,2009,47(4):860.
[26]	Yang S,Guo K,Li J,et al.Framework Formation of Financial Data Classification Standard in the Era of the Big Data[J].Procedia Computer Science,2014,30(0):88~96.
[27]	Rahimipanah M,Hamedi M,M M.Antioxidant activity and phenolic contents of Persian walnut (Juglans regia L.) green husk extract[J].Afr.J.Food Sci.Technol,2010,1(4):105~111.
[28]	李福荣,王庆国,韩纪举,等.青龙衣有效成分的初步提取分离及体外抗肿瘤活性研究[J].时珍国医国药,2011,22(3):608~609.
[29]	Alshatwi A A,Hasan T N,Shafi G,et al.Validation of the Antiproliferative Effects of Organic Extracts from the Green Husk of Juglans regia L.on PC-3 Human Prostate Cancer Cells by Assessment of Apoptosis-Related Genes.[J].Evidence-based Complementary & Alternative Medicine (eCAM),2012,2012(2):103026.
[30]	杨志宏.青龙衣粉针对肿瘤细胞抑制作用的实验研究[D].黑龙江省中医研究院,2003.
[31]	景炳年.核桃次生物质抗烟草花叶病毒活性的研究[D].西北农林科技大学,2007.
[32]	陈卫东,李建飞,吴桂军.核桃青皮萃取物防治板栗叶螨试验[J].河北果树,2009(5):8.
[33]	梁永锋.核桃青皮提取物对枸杞蚜虫的触杀和拒食活性研究[J].河南农业科学,2010,39(11):70~72.
[34]	梁永锋.核桃青皮提取物对萝卜蚜虫毒杀和拒食活性研究[J].江苏农业科学,2011,39(2):187~188.
[35]	李海洋.核桃青皮有效化学成分及抑菌性研究[D].西北农林科技大学,2012.
[36]	Cosmulescu S N,Trandafir I,Achim G,et al.Juglone content in leaf and green husk of five walnut (Juglans regia L.) cultivars.[J].Notulae Botanicae,Horti Agrobotanici,Cluj-Napoca,2011,39(39):237~240.
[37]	赵国建,席东亮,段江莲.核桃青皮多酚提取工艺优化[J].陕西农业科学,2013,59(04):3~5.
[38]	王红,李永霞,刘军海.超声波辅助提取核桃青皮中单宁的研究[J].现代农业,2011(08):81~85.
[39]	Fernándezagulló A,Pereira E,Freire M S,et al.Influence of solvent on the antioxidant and antimicrobial properties of walnut (Juglans regia L.) green husk extracts[J].Industrial Crops & Products,2013,42(1):126~132.
[40]	马良进,林君阳,李桥,等.山核桃外果皮中的抑菌活性成分[J].林业科学,2009,45(12):90~94.
[41]	赵国建,王向东,王焕.提取方法对核桃青皮多酚提取效果的影响[J].农业工程学报,2012(S1):351~355.
[42]	伏慧慧,谭梅,郭艳秋,等.响应面法优化"酶法-超声波"连续提取核桃青皮多酚[J].食品研究与开发,2015(7):42~47.
[43]	张旭,陈丹,曹丽娟,等.5种大孔树脂纯化鲜核桃青皮汁多酚工艺的比较[J].中成药,2016(08):1852~1855.
[44]	翟梅枝,郭琪,贾彩霞,等.大孔树脂分离纯化核桃青皮总黄酮的研究[J].生物质化学工程,2008(03):21~25.
[45]	马乐,韩军岐,白欢欢,等.采用大孔树脂分离纯化核桃青皮中多酚[J].食品与发酵工业,2016(03):237~242.

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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

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Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk

Sichuan Academy of Forestry, Chengdu 610081, China;Rongxian Forestry Bureau, Rongxian 43100;Chengdu 610068, China

Received Date: 2017-12-05

Key words:

Abstract: Walnut is one of the important forest products in our country.Polyphenolic compounds extracted from Walnut green husk were abundant and healthy to the human body.However because of carelessly discarded husk,environment became increasingly worsened.This paper reviewed the research progress of biological activity,separation and purification of the polyphenols of walnut green husk,and looked forward to the research and application in the future,aiming to provide some thoughts in scientific research and the application of walnut green husk's polyphenolic resources for the purpose of promoting the walnut industry.

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Reference (45)

[1]	郗荣庭,张毅萍.中国核桃[M].中国林业出版社,1992.
[2]	姚焕英,唐静成,张鞍灵,等.核桃属植物化学成分及生物活性研究[J].西北植物学报,2003,23(9):1650~1655.
[3]	周正.世界主要用材树种概论[M].中国林业出版社,1997.
[4]	Silva B M,Andrade P B,Valentão P,et al.Quince (Cydonia oblonga Miller) fruit (pulp,peel,and seed) and jam:antioxidant activity.[J].Journal of Agricultural & Food Chemistry,2004,52(15):4705.
[5]	Pulido R,Bravo L,Saura-Calixto F.Antioxidant activity of dietary polyphenols as determined by a modified ferric reducing/antioxidant power assay.[J].J Agric Food Chem,2000,48(8):3396~3402.
[6]	Stampar F,Solar A,Hudina M,et al.Traditional walnut liqueur-cocktail of phenolics.[J].Food Chemistry,2006,95(4):627~631.
[7]	杜旭,李玉文,倪雁,等.中药青核桃镇痛作用研究与展望[J].中国中药杂志,2000,25(1):7~10.
[8]	董再冉.核桃酒治疗腹痛和胃痛[J].中国医刊,1966(7	).
[9]	黄织女.青核桃泡酒治肺癌[J].老同志之友,2014(9):61.
[10]	林开敏,叶发茂,林艳,等.酚类物质对土壤和植物的作用机制研究进展[J].中国生态农业学报,2010,18(5):1130~1137.
[11]	何强,姚开,石碧.植物单宁的营养学特性[J].林产化学与工业,2001,21(1):80~85.
[12]	王全杰,李超,王纯,等.核桃青皮中单宁的类型及含量测定[J].皮革与化工,2011,28(3):25~27.
[13]	Binder R G,Benson M E,Flath R A.Eight 1,4-naphthoquinones from Juglans[J].Phytochemistry,1989,28(10):2799~2801.
[14]
[15]	Cushnie T P T,Lamb A J.Antimicrobial activity of flavonoids.International Journal of Antimicrobial Agents[J].2005(26):343~356
[16]	曲中原,邹翔,管小玉,等.青龙衣不同萃取部位化学成分GC-MS分析[J].中草药,2010,41(10):1625~1626.
[17]	Colaric M,Veberic R,Solar A,et al.Phenolic Acids,Syringaldehyde,and Juglone in Fruits of Different Cultivars of Juglans regia L.[J].Journal of Agricultural & Food Chemistry,2005,53(16):6390~6396.
[18]
[19]	张建斌,柳军玺,查飞,等.青龙衣的化学成分研究[J].中草药,2009,40(6):847~849.
[20]	Oliveira I,Sousa A,Ferreira I C,et al.Total phenols,antioxidant potential and antimicrobial activity of walnut (Juglans regia L.) green husks.[J].Food & Chemical Toxicology An International Journal Published for the British Industrial Biological Research Association,2008,46(7):2326.
[21]	Keskin D,Ceyhan N,Ugur A.Chemical composition and in vitro antimicrobial activity of walnut (Juglans regia) green husks and leaves from West Anatolia[J].Journal of Pure & Applied Microbiology,2012,6(2):583~588.
[22]	Pereira J A,Oliveira I,Sousa A,et al.Bioactive properties and chemical composition of six walnut (Juglans regia L.) cultivars.[J].Food & Chemical Toxicology,2008,46(6):2103~2111.
[23]	Yieit D,Yigit N,Aktas E,et al.Antimicrobial activity of walnut (Juglans regia L.)[J].Turk Microbiol Soc,2009,1~2(39):7~11.
[24]	Clark A M,Jurgens T M,Hufford C D.Antimicrobial activity of juglone.[J].Phytotherapy Research,1990,4(1):11~14.
[25]	Costa R M,Magalhães A S,Pereira J A,et al.Evaluation of free radical-scavenging and antihemolytic activities of quince (Cydonia oblonga) leaf:A comparative study with green tea (Camellia sinensis)[J].Food & Chemical Toxicology An International Journal Published for the British Industrial Biological Research Association,2009,47(4):860.
[26]	Yang S,Guo K,Li J,et al.Framework Formation of Financial Data Classification Standard in the Era of the Big Data[J].Procedia Computer Science,2014,30(0):88~96.
[27]	Rahimipanah M,Hamedi M,M M.Antioxidant activity and phenolic contents of Persian walnut (Juglans regia L.) green husk extract[J].Afr.J.Food Sci.Technol,2010,1(4):105~111.
[28]	李福荣,王庆国,韩纪举,等.青龙衣有效成分的初步提取分离及体外抗肿瘤活性研究[J].时珍国医国药,2011,22(3):608~609.
[29]	Alshatwi A A,Hasan T N,Shafi G,et al.Validation of the Antiproliferative Effects of Organic Extracts from the Green Husk of Juglans regia L.on PC-3 Human Prostate Cancer Cells by Assessment of Apoptosis-Related Genes.[J].Evidence-based Complementary & Alternative Medicine (eCAM),2012,2012(2):103026.
[30]	杨志宏.青龙衣粉针对肿瘤细胞抑制作用的实验研究[D].黑龙江省中医研究院,2003.
[31]	景炳年.核桃次生物质抗烟草花叶病毒活性的研究[D].西北农林科技大学,2007.
[32]	陈卫东,李建飞,吴桂军.核桃青皮萃取物防治板栗叶螨试验[J].河北果树,2009(5):8.
[33]	梁永锋.核桃青皮提取物对枸杞蚜虫的触杀和拒食活性研究[J].河南农业科学,2010,39(11):70~72.
[34]	梁永锋.核桃青皮提取物对萝卜蚜虫毒杀和拒食活性研究[J].江苏农业科学,2011,39(2):187~188.
[35]	李海洋.核桃青皮有效化学成分及抑菌性研究[D].西北农林科技大学,2012.
[36]	Cosmulescu S N,Trandafir I,Achim G,et al.Juglone content in leaf and green husk of five walnut (Juglans regia L.) cultivars.[J].Notulae Botanicae,Horti Agrobotanici,Cluj-Napoca,2011,39(39):237~240.
[37]	赵国建,席东亮,段江莲.核桃青皮多酚提取工艺优化[J].陕西农业科学,2013,59(04):3~5.
[38]	王红,李永霞,刘军海.超声波辅助提取核桃青皮中单宁的研究[J].现代农业,2011(08):81~85.
[39]	Fernándezagulló A,Pereira E,Freire M S,et al.Influence of solvent on the antioxidant and antimicrobial properties of walnut (Juglans regia L.) green husk extracts[J].Industrial Crops & Products,2013,42(1):126~132.
[40]	马良进,林君阳,李桥,等.山核桃外果皮中的抑菌活性成分[J].林业科学,2009,45(12):90~94.
[41]	赵国建,王向东,王焕.提取方法对核桃青皮多酚提取效果的影响[J].农业工程学报,2012(S1):351~355.
[42]	伏慧慧,谭梅,郭艳秋,等.响应面法优化"酶法-超声波"连续提取核桃青皮多酚[J].食品研究与开发,2015(7):42~47.
[43]	张旭,陈丹,曹丽娟,等.5种大孔树脂纯化鲜核桃青皮汁多酚工艺的比较[J].中成药,2016(08):1852~1855.
[44]	翟梅枝,郭琪,贾彩霞,等.大孔树脂分离纯化核桃青皮总黄酮的研究[J].生物质化学工程,2008(03):21~25.
[45]	马乐,韩军岐,白欢欢,等.采用大孔树脂分离纯化核桃青皮中多酚[J].食品与发酵工业,2016(03):237~242.

Progress of Research on the Active Ingredients,Separation and Purification of Walnut Green Husk

doi: 10.16779/j.cnki.1003-5508.2018.01.005

Abstract

References

Proportional views

通讯作者: 陈斌, bchen63@163.com

Related

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